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Fabrication of form stable NaCl-Al2O3 composite for thermal energy storage by cold sintering process

Bilyaminu Suleiman, Qinghua Yu, Yulong Ding, Yongliang Li

《化学科学与工程前沿（英文）》 2019年 第13卷 第4期   页码 727-735 doi: 10.1007/s11705-019-1823-2

摘要： A form stable NaCl-Al O (50-50 wt-%) composite material for high temperature thermal energy storage was fabricated by cold sintering process, a process recently applied to the densification of ceramics at low temperature ˂ 300°C under uniaxial pressure in the presence of small amount of transient liquid. The fabricated composite achieved as high as 98.65% of the theoretical density. The NaCl-Al O composite also retained the chloride salt without leakage after 30 heating-cooling cycles between 750°C–850°C together with a holding period of 24 h at 850°C. X-ray diffraction measurements indicated congruent solubility of the alumina in chloride salt, excellent compatibility of NaCl with Al O , and chemical stability at high temperature. Structural analysis by scanning electron microscope also showed limited grain growth, high density, uniform NaCl distribution and clear faceted composite structure without inter-diffusion. The latent heat storage density of 252.5 J/g was obtained from simultaneous thermal analysis. Fracture strength test showed high sintered strength around 5 GPa after 50 min. The composite was found to have fair mass losses due to volatilization. Overall, cold sintering process has the potential to be an efficient, safe and cost-effective strategy for the fabrication of high temperature thermal energy storage materials.

关键词： cold sintering process     composite fabrication     thermal energy storage     phase change materials    

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Simple fabrication of carboxymethyl cellulose and κ-carrageenan composite aerogel with efficient performance

《环境科学与工程前沿（英文）》 2022年 第16卷 第10期 doi: 10.1007/s11783-022-1568-x

摘要：

● A composite aerogel was simply obtained to remove various fluoroquinolones (FQs).

关键词： Composite aerogel of carboxymethyl cellulose and κ-carrageenan     Fluoroquinolone antibiotics     Adsorption performance     Coexisting substances     Adsorption mechanism     Reusability    

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One-pot hydrothermal fabrication of BiVO/FeO/rGO composite photocatalyst for the simulated solar light-driven

《环境科学与工程前沿（英文）》 2022年 第16卷 第3期 doi: 10.1007/s11783-021-1470-y

摘要：

• BiVO4/Fe3O4/rGO has excellent photocatalytic activity under solar light radiation.

关键词： Photocatalysis     Ternary magnetic photocatalyst     Visible-light-driven     Free radicals trapping     Reusability     Recycling    

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Fabrication of magnetic multi-template molecularly imprinted polymer composite for the selective and

《环境科学与工程前沿（英文）》 2021年 第15卷 第5期 doi: 10.1007/s11783-021-1395-5

摘要：

• Magnetic multi-template molecularly imprinted polymer composite was synthesized.

关键词： Tetracyclines     Removal     Adsorption     Molecularly imprinted polymer     Magnetic graphene oxide    

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Fabrication of high-performance pervaporation composite membrane for alkaline wastewater reclamation

《化学科学与工程前沿（英文）》 2022年 第16卷 第5期   页码 709-719 doi: 10.1007/s11705-021-2078-2

摘要： Pervaporation desalination has a unique advantage to recycle concentrated salt solutions. The merit can be applied to treat alkaline wastewater if the membrane has superior alkali-resistance. In this paper, we used polyethylene microfiltration membrane as the substrate and deposited a glutaraldehyde crosslinked sodium carboxymethylcellulose layer by spray-coating. Pervaporation flux of the composite membrane reached 35€±€2 kg·m–2·h–1 with a sodium chloride rejection of 99.9%€±€0.1% when separating a 3.5 wt-% sodium chloride solution at 70 °C. The desalination performance was stable after soaking the membrane in a 20 wt-% NaOH solution at room temperature for 9 d and in a 10 wt-% NaOH solution at 60 °C for 80 h. Moreover, the membrane was stable in 4 wt-% sulfuric acid and a 500 mg·L−1 sodium hypochlorite solution. In a process of concentrating a NaOH solution from 5 to 10 wt-% at 60 °C, an average water flux of 23 kg·m–2·h–1 with a NaOH rejection over 99.98% was obtained.

关键词： pervaporation     alkaline solution concentration     polyethylene membrane     acid resistance     chlorine tolerance    

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Facile fabrication of dolomite-doped biochar/bentonite for effective removal of phosphate from complex

《环境科学与工程前沿（英文）》 2023年 第17卷 第6期 doi: 10.1007/s11783-023-1671-7

摘要：

● Dolomite-doped biochar/bentonite was synthesized for phosphate removal.

关键词： Biochar-bentonite composite     Dolomite doping     Phosphate adsorption     Polymeric matrix membrane     Adsorption-filtration dual functions     Low-concentration phosphate    

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Fabrication of titania thin film with composite nanostructure and its ability to photodegrade rhodamine

ZHANG Gaojie, WU Jinming, LIU Shaoguang, YAN Mi

《化学科学与工程前沿（英文）》 2008年 第2卷 第1期   页码 44-48 doi: 10.1007/s11705-008-0001-8

摘要： A titania nanorod film was synthesized by direct oxidation of metallic Ti with hydrogen peroxide solution under a low temperature. Titania nanoparticles were then filled into the gaps among the nanorods through an infiltration sol-gel procedure to form a composite titania film with an ordered nanostructure. X-ray diffraction spectra indicate that the composite film was a mixture of anatase and rutile while the titania film obtained by only using a sol-gel procedure was pure anatase. Field emission scanning electron microscopy observations show that titania nanoparticles were embedded into the titania nanorod film. Photoluminescence spectra suggest the enhanced separation of electron and hole pairs for the obtained composite titania film over the corresponding titania nanorod film. The composite titania film exhibited improved ability to photodegrade rhodamine B in water compared with the titania nanorod film. The apparent photodegradation rate constant, fitting a pseudo-first-order, was 3 times of that obtained by the sol-gel derived titania film at the same weight. The improved photocatalytic activity for the composite titania film could be attributed to the enhanced separation of electron and hole pairs due to the embedding of the titania nanoparticles within the titania nanorods.

关键词： constant     weight     apparent photodegradation     hydrogen     nanorod    

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多相复合陶瓷刀具材料的设计与制备

许崇海,艾兴

《中国工程科学》 2001年 第3卷 第3期   页码 71-74

摘要：

陶瓷材料的多相复合与计算机辅助设计是21世纪先进陶瓷材料的重要发展趋势。文章采用理论与实验相结合的方法，建立了多相复合陶瓷刀具材料力学性能与材料组分之间关系的数学模型，采用计算机辅助优 化设计技术求得材料的最优组分。在此基础上，利用热压技术制得一种Al2〇3-SiC-(W,Ti) C多相复合陶瓷刀具材料，该材料具有良好的综合力学性能。

关键词： 陶瓷刀具材料     多相复合     材料设计     模型     力学性能    

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Fabrication and performance of PEN SOFCs with proton-conducting electrolyte

ZHONG Li, LUO Jingli, Karl Chuang

《化学科学与工程前沿（英文）》 2007年 第1卷 第1期   页码 40-44 doi: 10.1007/s11705-007-0008-6

摘要： A positive-electrolyte-negative (PEN) assembly solid oxide fuel cell (SOFC) with a thin electrolyte film for intermediate temperature operation was fabricated. Instead of the traditional screen-printing method, both anode and cathode catalysts were pressed simultaneously and formed with the fabrication of nano-composite electrolyte by press method. This design offered some advantageous configurations that diminished ohmic resistance between electrolyte and electrodes. It also increased the proton-conducting rate and improved the performance of SOFC due to the reduction of membrane thickness and good contact between electrolyte and electrodes. The fabricated PEN cell generated electricity between 600?C and 680?C using HS as fuel feed and air as oxidant. Maximum power densities 40 mW " cm and 130 mW " cm for the PEN configuration with a Mo-Ni-S-based composite anode, nano-composite electrolyte (LiSO+AlO) film and a NiO-based composite cathode were achieved at 600?C and 680?C, respectively.

关键词： proton-conducting     positive-electrolyte-negative     temperature operation     Mo-Ni-S-based composite     advantageous    

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Mesoscale fabrication of a complex surface for integral impeller blades

Xibin WANG,Tianfeng ZHOU,Lijing XIE,Li JIAO,Zhibing LIU,Zhiqiang LIANG,Pei YAN

《机械工程前沿（英文）》 2017年 第12卷 第1期   页码 116-131 doi: 10.1007/s11465-017-0426-1

摘要：

Integral impeller is the most important component of a mini-engine. However, the machining of a mesoscale impeller with a complex integral surface is difficult because of its compact size and high accuracy requirement. A mesoscale component is usually manufactured by milling. However, a conventional milling tool cannot meet the machining requirements because of its size and stiffness. For the fabrication of a complex integral impeller, a micro-ball-end mill is designed in accordance with the non-instantaneous-pole envelope principle and manufactured by grinding based on the profile model of the helical groove and the mathematical model of the cutting edge curve. Subsequently, fractal theory is applied to characterize the surface quality of the integral impeller. The fractal theory-based characterization shows that the completed mesoscale integral impeller exhibits a favorable performance in terms of mechanical properties and morphological accuracy.

关键词： mesoscale fabrication     micro-milling tool     mesoscale milling     impeller blade    

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用于电热转换、电磁屏蔽的导电陶瓷的简易大规模制备 Article

李岱祺, 唐彬, 程德山, 吴静, 唐文杨, 赵仲, 李建强, 蔡光明, 王金凤, 王训该

《工程（英文）》 2023年 第21卷 第2期   页码 143-151 doi: 10.1016/j.eng.2021.12.017

摘要：

通过传统瓷砖制备工艺的干压法，制备了一种碳化酚醛树脂基导电陶瓷复合材料（CCC）。首先，将导电前驱体溶液（酚醛树脂）与陶瓷前驱体均匀混合，随后在单次热处理中同时实现了碳化和陶瓷化。碳化后的材料赋予复合材料出色的电导率和可靠的循环加热特性。在12 V电压下通电10 min 后材料表面温度可达386 ℃，在20 V电压下达到400 ℃仅需48 s。红外热像图表明，热量在复合材料表面分布均匀，并且可以通过更改电路布置（串联或并联）来调节电热转换性能。此外，与普通陶瓷相比，导电陶瓷复合材料在8.2 GHz下表现出了26.2 dB的优异电磁屏蔽性能，并提升了光热转换性能。更重要的是，这种单次热处理加热生产导电陶瓷复合材料的方法成本较低，可在原有瓷砖生产线的基础上进行大规模生产。出色的电学性能促进了该陶瓷复合材料在焦耳加热（如除冰、烧水和烹饪）及电磁屏蔽中的应用。

关键词： 导电陶瓷复合材料     电热转换性能     电磁屏蔽     碳化    

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超疏水SiO2/PS 薄膜于木材表面的构建

张明,王成毓

《中国工程科学》 2014年 第16卷 第4期   页码 83-86

摘要：

通过溶胶-凝胶法一步合成疏水性且具备独特形貌的二氧化硅粒子，联合聚苯乙烯以滴涂的方式 于木材表面仿生合成了稳定性超疏水薄膜。经处理后的木材表面与水的静态接触角为153°，滚动角小于5°。通过扫描电子显微镜照片观察到该复合涂层拥有微米/亚微米的二维等级粗糙结构，该结构协同低表面能物质共同决定超疏水性木材的成功制得。此外，进一步研究了超疏水性木材表面的稳定性和耐久性。结果表明，该超疏水性木材于水、腐蚀性液体（酸液/碱液）、常见有机溶剂中以及一些常见条件下仍保留超疏水特性，为未来木材材料的应用领域扩展提供了有利条件。

关键词： 超疏水     木材表面     滴涂法     复合薄膜    

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A multi-probe micro-fabrication apparatus based on the friction-induced fabrication method

Zhijiang WU, Chenfei SONG, Jian GUO, Bingjun YU, Linmao QIAN

《机械工程前沿（英文）》 2013年 第8卷 第4期   页码 333-339 doi: 10.1007/s11465-013-0276-4

摘要：

A novel multi-probe micro-fabrication apparatus was developed based on the friction-induced fabrication method. The main parts of the apparatus include actuating device, loading system, and control system. With a motorized linear stage, the maximum fabrication area of 50 mm × 50 mm can be achieved, and the maximum sliding speed of probes can be as high as 10 mm/s. Through locating steel micro balls into indents array, the preparation of multi-probe array can be realized by a simple and low-cost way. The cantilever was designed as a structure of deformable parallelogram with two beams, by which the fabrication force can be precisely controlled. Combining the friction-induced scanning with selective etching in KOH solution, various micro-patterns were fabricated on Si(100) surface without any masks or exposure. As a low-cost and high efficiency fabrication device, the multi-probe micro-fabrication apparatus may encourage the development of friction-induced fabrication method and shed new light on the texture engineering.

关键词： friction-induced fabrication     silicon     surface texture     friction     multi-probe    

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Precision glass molding: Toward an optimal fabrication of optical lenses

Liangchi ZHANG,Weidong LIU

《机械工程前沿（英文）》 2017年 第12卷 第1期   页码 3-17 doi: 10.1007/s11465-017-0408-3

摘要：

It is costly and time consuming to use machining processes, such as grinding, polishing and lapping, to produce optical glass lenses with complex features. Precision glass molding (PGM) has thus been developed to realize an efficient manufacture of such optical components in a single step. However, PGM faces various technical challenges. For example, a PGM process must be carried out within the super-cooled region of optical glass above its glass transition temperature, in which the material has an unstable non-equilibrium structure. Within a narrow window of allowable temperature variation, the glass viscosity can change from 105 to 1012 Pa·s due to the kinetic fragility of the super-cooled liquid. This makes a PGM process sensitive to its molding temperature. In addition, because of the structural relaxation in this temperature window, the atomic structure that governs the material properties is strongly dependent on time and thermal history. Such complexity often leads to residual stresses and shape distortion in a lens molded, causing unexpected changes in density and refractive index. This review will discuss some of the central issues in PGM processes and provide a method based on a manufacturing chain consideration from mold material selection, property and deformation characterization of optical glass to process optimization. The realization of such optimization is a necessary step for the Industry 4.0 of PGM.

关键词： precision glass molding     optical lens     constitutive modeling     optimization     manufacturing chain     Industry 4.0    

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Technological development and engineering applications of novel steel-concrete composite structures

Jianguo NIE, Jiaji WANG, Shuangke GOU, Yaoyu ZHU, Jiansheng FAN

《结构与土木工程前沿（英文）》 2019年 第13卷 第1期   页码 1-14 doi: 10.1007/s11709-019-0514-x

摘要：

In view of China’s development trend of green building and building industrialization, based on the emerging requirements of the structural engineering community, the development and proposition of novel resource-saving high-performance steel-concrete composite structural systems with adequate safety and durability has become a kernel development trend in structural engineering. This paper provides a state of the art review of China’s cutting-edge research and technologies in steel-concrete composite structures in recent years, including the building engineering, the bridge engineering and the special engineering. This paper summarizes the technical principles and applications of the long-span bi-directional composite structures, the long-span composite transfer structures, the comprehensive crack control technique based on uplift-restricted and slip-permitted (URSP) connectors, the steel plate concrete composite (SPCC) strengthen technique, and the innovative composite joints. By improving and revising traditional structure types, the comprehensive superiority of steel-concrete composite structures is well elicited. The research results also indicate that the high-performance steel-concrete composite structures have a promising popularizing prospect in the future.

关键词： high-performance composite structure     bi-directional composite     composite transfer     uplift-restricted and slip-permitted connectors     steel plate concrete composite strengthen    

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标题 作者 时间 类型 操作

Fabrication of form stable NaCl-Al2O3 composite for thermal energy storage by cold sintering process

Bilyaminu Suleiman, Qinghua Yu, Yulong Ding, Yongliang Li

期刊论文

Simple fabrication of carboxymethyl cellulose and κ-carrageenan composite aerogel with efficient performance

期刊论文

One-pot hydrothermal fabrication of BiVO/FeO/rGO composite photocatalyst for the simulated solar light-driven

期刊论文

Fabrication of magnetic multi-template molecularly imprinted polymer composite for the selective and

期刊论文

Fabrication of high-performance pervaporation composite membrane for alkaline wastewater reclamation

期刊论文

Facile fabrication of dolomite-doped biochar/bentonite for effective removal of phosphate from complex

期刊论文

Fabrication of titania thin film with composite nanostructure and its ability to photodegrade rhodamine

ZHANG Gaojie, WU Jinming, LIU Shaoguang, YAN Mi

期刊论文

多相复合陶瓷刀具材料的设计与制备

许崇海,艾兴

期刊论文

Fabrication and performance of PEN SOFCs with proton-conducting electrolyte

ZHONG Li, LUO Jingli, Karl Chuang

期刊论文

Mesoscale fabrication of a complex surface for integral impeller blades

Xibin WANG,Tianfeng ZHOU,Lijing XIE,Li JIAO,Zhibing LIU,Zhiqiang LIANG,Pei YAN

期刊论文

用于电热转换、电磁屏蔽的导电陶瓷的简易大规模制备

李岱祺, 唐彬, 程德山, 吴静, 唐文杨, 赵仲, 李建强, 蔡光明, 王金凤, 王训该

期刊论文

超疏水SiO2/PS 薄膜于木材表面的构建

张明,王成毓

期刊论文

A multi-probe micro-fabrication apparatus based on the friction-induced fabrication method

Zhijiang WU, Chenfei SONG, Jian GUO, Bingjun YU, Linmao QIAN

期刊论文

Precision glass molding: Toward an optimal fabrication of optical lenses

Liangchi ZHANG,Weidong LIU

期刊论文

Technological development and engineering applications of novel steel-concrete composite structures

Jianguo NIE, Jiaji WANG, Shuangke GOU, Yaoyu ZHU, Jiansheng FAN

期刊论文